GB/T 46611-2025 Lithium niobate single-crystal thin film for electro-optic modulator English, Anglais, Englisch, Inglés, えいご
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ICS 13.220.10
CCS H 57
National Standard of the People's Republic of China
GB/T 46609-2025
Lithium niobate single-crystal thin film for electro-optic modulator
电光调制器用铌酸锂单晶薄膜
Issue date: 2025-10-31 Implementation date: 2026-05-01
Issued by the General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China
the Standardization Administration of the People's Republic of China
Contents
Foreword
1 Scope
2 Normative References
3 Terms and Definitions
4 Requirements
4.1 Appearance Quality
4.2 Tolerance of Surface Orientation
4.3 Tolerance of Bonding Deflection Angle
4.4 Bonding Strength
4.5 Optical Homogeneity
4.6 Linear Electro-Optic Coefficient
4.7 Single-Domain Degree
4.8 Substrate Resistivity
5 Test Methods
5.1 Test Environment
5.2 Total Thickness
5.3 Total Thickness Variation
5.4 Local Thickness Variation and Percent Local Thickness Variation
5.5 Edge Area Width
5.6 Surface Appearance Quality
5.7 17-Point Average Thickness Tolerance and 17-Point Thickness Variation
5.8 Bow
5.9 Front Surface Roughness
5.10 Tolerance of Surface Orientation
5.11 Tolerance of Bonding Deflection Angle
5.12 Bonding Strength
5.13 Optical Homogeneity
5.14 Linear Electro-Optic Coefficient
5.15 Single-Domain Degree
5.16 Substrate Resistivity
6 Inspection and Acceptance Rules
6.1 Inspection and Acceptance
6.2 Inspection Categories
6.3 Inspection Items
6.4 Lot Inspection
6.5 Periodic Inspection
7 Packaging, Labeling/Marking, Storage and Transport
7.1 Packaging
7.2 Labeling/Marking
7.3 Storage
7.4 Transport
Appendix A (Normative) Method for Measuring Bonding Deflection Angle
Appendix B (Normative) Method for Measuring Optical Homogeneity
Appendix C (Normative) Method for Measuring Linear Electro-Optic Coefficient
Appendix D (Normative) Method for Measuring Single-Domain Degree
1 Scope
This document specifies the requirements, inspection and testing rules, packaging, labeling/marking, storage, and transportation requirements for lithium niobate single-crystal thin films used in electro-optic modulators. It also describes the test methods.
This document applies to congruently-melt lithium niobate single-crystal thin films for electro-optic modulators with X-cut orientation, a lithium niobate thin film layer thickness ranging from 100 nm to 1,000 nm, and diameters of 76.2 mm, 100.0 mm, 150.0 mm, and 200.0 mm. Lithium niobate single-crystal thin films of other specifications may refer to this document for implementation.
2 Normative References
The following documents contain provisions that, through normative reference in this text, constitute essential provisions of this document. For dated references, only the edition corresponding to that date applies. For undated references, the latest edition of the referenced document (including any amendments) applies.
GB/T 191-2008 Packaging—Pictorial marking for handling of goods
GB/T 1185 Surface imperfections of optical parts
GB/T 1551 Test method for resistivity of silicon single crystal—Two-probe and four-probe D. C. methods on straight specimens
GB/T 2828.1-2012 Sampling procedures for inspection by attributes—Part 1: Sampling schemes indexed by acceptance quality limit (AQL) for lot-by-lot inspection
GB/T 6618 Test method for thickness and total thickness variation of silicon slices
GB/T 6619 Test method for bow of silicon slices
GB/T 14264 Terminology of semiconductor materials
GB/T 20919 Digital external micrometer
GB/T 25915.1-2021 Cleanrooms and associated controlled environments—Part 1: Classification of air cleanliness by particle concentration
GB/T 29505 Test method for measuring surface roughness on planar surfaces of silicon wafers
GB/T 30118 Specification and measuring method of single crystal wafer for surface acoustic wave (SAW) devices
GB/T 30857 Test method for thickness and thickness variation of sapphire substrates
GB/T 40279 Test method for thin film thickness on silicon wafer surfaces—Optical reflectance method
GB/T 41853 Semiconductor devices—Micro-electromechanical devices—Measurement of bonding strength between wafers
3 Terms and Definitions
For the purposes of this document, the terms and definitions given in GB/T 14264, GB/T 6619, GB/T 30118, and the following apply.
3.1
lithium niobate single-crystal thin film; TFLN
A thin film compound of single-crystal lithium niobate with the chemical formula LiNbO₃, prepared on a specific substrate, with a thickness ranging from 100 nm to 1,000 nm.
Note: TFLN typically comprises a sequentially stacked structure of a lithium niobate single-crystal thin film layer, an insulating layer, a trap layer, and a substrate. The trap layer may be omitted as required. Its structure is shown in Figure 1.
3.3
average thickness tolerance of 17 positions; TT17
The allowable tolerance for the average thickness of each film layer measured at 17 specified positions.
3.4
thickness variation of 17 positions; TV17
The degree of variation in the thickness of each film layer measured at 17 specified positions, defined as the difference between the maximum and minimum values among the 17 thickness measurements.
3.5
total thickness variation; TTV
The deviation between the maximum and minimum thickness of the TFLN.
3.6
local thickness variation; LTV
The thickness variation within a matrix formed by selected areas of specific side lengths on the TFLN.
3.7
percent local thickness variation; PLTV
The percentage of the selected areas that satisfy the specified LTV value.
3.8
edge area
The region at the edge of the TFLN where the lithium niobate single-crystal thin film layer is absent.
Note: Its dimension is defined as the distance between the edge of the lithium niobate single-crystal thin film layer and the edge of the substrate, referred to as the edge area width.
3.9
fixed quality area; FQA
The inner region of the TFLN determined by a distance of 5 mm from the edge of the TFLN substrate, as shown in Figure 2.
3.10
tolerance of surface orientation
The allowable tolerance between the specified surface orientation of the lithium niobate single-crystal thin film layer and the measured orientation obtained through X-ray diffraction.
3.11
tolerance of bonding deflection angle
The allowable tolerance for the angle between the orientation flat of the lithium niobate single-crystal thin film layer and the orientation flat of the substrate in the TFLN.
3.12
void
A region within the TFLN where the lithium niobate single-crystal thin film layer or the insulating layer is missing.
3.13
colour spot
A region on the surface of the lithium niobate single-crystal thin film layer exhibiting color variation.
4 Requirements
4.1 Appearance and Quality
4.1.1 Dimensions of TFLN
The dimensional and tolerance technical requirements for TFLN shall comply with the provisions of Table 1.
Table 1 Technical Requirements for Dimensions and Tolerances of TFLN
4.2 Tolerance of Surface Orientation
Shall be not greater than 0.3°.
4.3 Tolerance of Bonding Deflection Angle
Shall be not greater than 1°.